Abstract Different bis-phenols reacted with cyanogen bromide in the presence of triethylamine as base to give the corresponding bis-cyanates which were treated with sodium azide in acetone as solvent to produce new bis (5-oxy-1 H-tetrazole) derivatives. One more bis-tetrazole derivative was synthesized by reaction of 5-(4-aminophenoxy)-1 H- tetrazole with adipoyl chloride. The prepared compounds were characterized by usual ...