Tetrahedron

An alternative synthesis of unsaturated aldehydopheromones

D Becker, T Kimmel

Index: Becker, D.; Kimmel, T. Tetrahedron, 1982 , vol. 38, # 11 p. 1689 - 1692

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Abstract

... Glc Column B flow 1 ml/min/150 retention time 72 min. D. BECKER and T. KIMMEL Heneicosa-7(E), 14(8)-diene 6 5 g of diyne 1 (17.4 mmol) were dissolved in 100 ml of diglyme, added dropwise to 10 g lithium aluminium hydride in 50 ml of diglyme and refluxed for 24 h. To the reaction mixture were added 200 ml of 10% hydrochloric acid and 300 ml of water, and the organic compound was extracted with 250 ml hexane. ...