e.g. Filippa Pettersson or Cancer Res. 75(6) , 1102-12, (2015) or 10.1002/anie.201600521
A straightforward synthetic approach for roxindole
JHM Lange, JC de Jong, HJ Sanders, GM Visser…
Index: Lange, Jos H. M.; De Jong, Johannes C.; Sanders, Hans J.; Visser, Geb M.; Kruse, Chris G. Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 7 p. 1055 - 1056
A concise synthetic approach to the dopamine autoreceptor agonist roxindole 1 has been devised. The key step in the novel route is the addition of succinic anhydride to 5- methoxyindolylmagnesium bromide, which circumvents the cumbersome construction of the indole moiety—via the Japp Klingemann-Fischer indole methodology—in the original route. This novel route will enable a quick, multi-gram synthesis of roxindole from cheap starting ...