A Practical, Automated Synthesis of meta-[18F] Fluorobenzylguanidine for Clinical Use

B Hu, AL Va̅vere, KD Neumann…

Index: Landge, Kamalkishor P.; Jang, Keun Sam; Lee, Sang Yeul; Chi, Dae Yoon Journal of Organic Chemistry, 2012 , vol. 77, # 13 p. 5705 - 5713

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Citation Number: 1

Abstract

... Neurosci. All Publications/Website. Select a Journal or Book ... of Chemistry, University of Nebraska−Lincoln, Lincoln, Nebraska 68588, United States. § Division of Nuclear Medicine, Department of Diagnostic Imaging, St. ... ACS Chem. Neurosci. ...

 Related Synthetic Route
(2-Iodophenyl)methanol Structure

5159-41-1

(2-Iodophenyl)m...

~95%

α-Bromo-2-iodotoluene Structure

40400-13-3

α-Bromo-2-iodot...

(2-(2-(t-butoxycarbonylamino)ethyl)phenyl)(4-fluorophenyl)iodonium p-toluenesulfonate Structure

1382354-94-0

(2-(2-(t-butoxy...

~82%

1-BOC-INDOLINE Structure

143262-10-6

1-BOC-INDOLINE

(2-(2-(t-butoxycarbonylamino)ethyl)phenyl)(4-chlorophenyl)iodonium p-toluenesulfonate Structure

1382354-96-2

(2-(2-(t-butoxy...

~80%

1-BOC-INDOLINE Structure

143262-10-6

1-BOC-INDOLINE

(2-(2-(t-butoxycarbonylamino)ethyl)phenyl)(4-bromophenyl)iodonium p-toluenesulfonate Structure

1382354-98-4

(2-(2-(t-butoxy...

~76%

1-BOC-INDOLINE Structure

143262-10-6

1-BOC-INDOLINE

(2-(2-(t-butoxycarbonylamino)ethyl)phenyl)(4-methoxyphenyl)iodonium p-toluenesulfonate Structure

1382355-00-1

(2-(2-(t-butoxy...

~72%

1-BOC-INDOLINE Structure

143262-10-6

1-BOC-INDOLINE

(2-(2-(t-butoxycarbonylamino)ethyl)phenyl)(p-tolyl)iodonium p-toluenesulfonate Structure

1382355-02-3

(2-(2-(t-butoxy...

~71%

1-BOC-INDOLINE Structure

143262-10-6

1-BOC-INDOLINE

t-butyl 2-[2-(trimethylstannyl)phenyl]ethylcarbamate Structure

1382354-89-3

t-butyl 2-[2-(t...

~%

1-BOC-INDOLINE Structure

143262-10-6

1-BOC-INDOLINE

(2-Iodophenyl)methanol Structure

5159-41-1

(2-Iodophenyl)m...

~%

(2-Iodophenyl)acetonitrile Structure

40400-15-5

(2-Iodophenyl)a...

sodium cyanide Structure

773837-37-9

sodium cyanide

α-Bromo-2-iodotoluene Structure

40400-13-3

α-Bromo-2-iodot...

~90%

(2-Iodophenyl)acetonitrile Structure

40400-15-5

(2-Iodophenyl)a...

(2-(2-(3,3-diethylureido)ethyl)phenyl)(4-fluorophenyl)iodonium p-toluenesulfonate Structure

1382355-24-9

(2-(2-(3,3-diet...

~67%

N,N-diethyl-2,3-dihydroindole-1-carboxamide Structure

61589-12-6

N,N-diethyl-2,3...

1,1-diethyl-3-[2-(2-trimethylstannylphenyl)]ethylurea Structure

1382354-92-8

1,1-diethyl-3-[...

~%

N,N-diethyl-2,3-dihydroindole-1-carboxamide Structure

61589-12-6

N,N-diethyl-2,3...

1-Chloro-4-iodobenzene Structure

637-87-6

1-Chloro-4-iodo...

Sodium acetate Structure

127-09-3

Sodium acetate

~64%

[acetyloxy-(4-chlorophenyl)-λ3-iodanyl] acetate Structure

6973-73-5

[acetyloxy-(4-c...

(2-(2-acetamidoethyl)phenyl)(4-fluorophenyl)iodonium p-toluenesulfonate Structure

1382355-14-7

(2-(2-acetamido...

~73%

1-Acetylindoline Structure

16078-30-1

1-Acetylindoline


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