2-Amino-5-bromophenol

Published date: 2022-11-17 14:20:02

2-Amino-5-bromophenol Structure
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Name 2-Amino-5-bromophenol CAS# 38191-34-3
Price ¥Inquiry/1kg ¥Inquiry/99kg ¥Inquiry/499kg ¥Inquiry/999kg Purity 99.9%
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General procedure: To a solution of o-aminophenol (400 mg, 3.67 mmol) and NCTS (998 mg, 3.67 mmol) in THF (6 mL), 1 M LiHMDS in hexane (3.67 mL, 3.67 mmol) was added and stirred at 5 °C to r.t. for 1h. Then the reaction mixture was poured in ice water and stirred for 15 min. Then extracted with EtOAc, the organic layer was separated. The organic layer was washed with brine solution.Then organic layer was dried over Na2SO4, filtered, and concentrated under reduced pressure. The crude product was purified by silica gel column chromatography to obtained pure 2-aminobenzaxozole in 90percent yield (471 mg).

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Hebei Xinsheng New Material Technology Co. LTD

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Tel: 86-16632313095
Address: No. 568, Gucheng Ying Town Industrial Zone, Qiu County, Handan City, Hebei Province
Area: China
Contact: lulu
Contact Phone #: 16632313095
Email: xinsheng03@xsmaterial.com
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