1H-Phosphole,2,5-dihydro-1-methoxy-3-methyl-, 1-oxide

Modify Date: 2024-01-10 20:34:01

1H-Phosphole,2,5-dihydro-1-methoxy-3-methyl-, 1-oxide Structure
1H-Phosphole,2,5-dihydro-1-methoxy-3-methyl-, 1-oxide structure
 Common Name 1H-Phosphole,2,5-dihydro-1-methoxy-3-methyl-, 1-oxide
CAS Number 695-59-0 Molecular Weight 146.12400
Density 1.08g/cm3 Boiling Point 192.5ºC at 760 mmHg
Molecular Formula C6H11O2P Melting Point N/A
MSDS N/A Flash Point 84.5ºC

 Names

Name 1-methoxy-3-methyl-2,5-dihydro-1λ5-phosphole 1-oxide
Synonym More Synonyms

 Chemical & Physical Properties

Density 1.08g/cm3
Boiling Point 192.5ºC at 760 mmHg
Molecular Formula C6H11O2P
Molecular Weight 146.12400
Flash Point 84.5ºC
Exact Mass 146.05000
PSA 36.11000
LogP 1.87080
Index of Refraction 1.446

 Toxicological Information

CHEMICAL IDENTIFICATION

RTECS NUMBER :
SZ6103800
CHEMICAL NAME :
3-Phospholene, 1-methoxy-3-methyl-, 1-oxide
CAS REGISTRY NUMBER :
695-59-0
LAST UPDATED :
199612
DATA ITEMS CITED :
1
MOLECULAR FORMULA :
C6-H11-O2-P

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Intraperitoneal
SPECIES OBSERVED :
Rodent - mouse
DOSE/DURATION :
3250 mg/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
REFERENCE :
DANKAS Doklady Akademii Nauk SSSR. Proceedings of the Academy of Sciences of the USSR. For English translation, see DBIOAM and DKBSAS. (V/O Mezhdunarodnaya Kniga, 113095 Moscow, USSR) V.1- 1933- Volume(issue)/page/year: 160,826,1965

 Synthetic Route

Methanol structure

Methanol

CAS#:67-56-1
1-hydroxy-3-methyl-2,5-dihydro-1λ5-phosphole 1-oxide structure

1-hydroxy-3-met...

CAS#:87243-93-4

~78%

1H-Phosphole,2,5-dihydro-1-methoxy-3-methyl-, 1-oxide Structure

1H-Phosphole,2,...

CAS#:695-59-0
Literature: Jablonkai, Erzsebet; Milen, Matyas; Drahos, Laszlo; Keglevich, Gyoergy Tetrahedron Letters, 2013 , vol. 54, # 44 p. 5873 - 5875
Methanol structure

Methanol

CAS#:67-56-1
1-chloro-3-methyl-2,5-dihydro-1λ5-phosphole 1-oxide structure

1-chloro-3-meth...

CAS#:18874-22-1

~77%

1H-Phosphole,2,5-dihydro-1-methoxy-3-methyl-, 1-oxide Structure

1H-Phosphole,2,...

CAS#:695-59-0
Literature: Keglevich, Gyoergy; Petnehazy, Imre; Miklos, Peter; Almasy, Attila; Toth, Gabor; et al. Journal of Organic Chemistry, 1987 , vol. 52, # 18 p. 3983 - 3986
2,3,7-Trimethyl-5-methoxy-1,4,5-dioxaphosphaspiro[4,4]nona-2,7-diene structure

2,3,7-Trimethyl...

CAS#:102639-94-1

~67%

3-methoxybutan-2-one structure

3-methoxybutan-2-one

CAS#:17742-05-1
1H-Phosphole,2,5-dihydro-1-methoxy-3-methyl-, 1-oxide Structure

1H-Phosphole,2,...

CAS#:695-59-0
Literature: Arbuzov, B. A.; Vizel', A. O.; Shchukina, L. I.; Vakulenko, O. V.; Zyablikova, T. A.; et al. J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 8 p. 1705 - 1709,1514 - 1518
Methanol structure

Methanol

CAS#:67-56-1
2,3,7-Trimethyl-5-methoxy-1,4,5-dioxaphosphaspiro[4,4]nona-2,7-diene structure

2,3,7-Trimethyl...

CAS#:102639-94-1

~65%

3-methoxybutan-2-one structure

3-methoxybutan-2-one

CAS#:17742-05-1
1H-Phosphole,2,5-dihydro-1-methoxy-3-methyl-, 1-oxide Structure

1H-Phosphole,2,...

CAS#:695-59-0
Literature: Arbuzov, B. A.; Vizel', A. O.; Shchukina, L. I.; Vakulenko, O. V.; Zyablikova, T. A.; et al. J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 8 p. 1705 - 1709,1514 - 1518
1-Methoxy-3-methyl-3-phospholene structure

1-Methoxy-3-met...

CAS#:50982-84-8

~%

1H-Phosphole,2,5-dihydro-1-methoxy-3-methyl-, 1-oxide Structure

1H-Phosphole,2,...

CAS#:695-59-0
Literature: Arbuzov, B. A.; Vizel', A. O.; Shchukina, L. I.; Vakulenko, O. V.; Zyablikova, T. A.; et al. J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 8 p. 1705 - 1709,1514 - 1518
Methanol structure

Methanol

CAS#:67-56-1
1-(2-chloroethoxy)-3-methylphosphol-3-ene structure

1-(2-chloroetho...

CAS#:50982-88-2

~%

1-ethyl-3-methyl-2,5-dihydro-1λ5-phosphole 1-oxide structure

1-ethyl-3-methy...

CAS#:7529-24-0
1,3-Dimethyl-2,5-dihydro-1H-phosphole 1-oxide structure

1,3-Dimethyl-2,...

CAS#:15450-79-0
Detail
Literature: Arbuzov, B. A.; Vizel', A. O.; Shchukina, L. I.; Giniyatullin, R. S. Doklady Chemistry, 1980 , vol. 253, p. 371 - 374 Dokl. Akad. Nauk SSSR Ser. Khim., 1980 , vol. 253, # 4 p. 879 - 883
Bromoethane structure

Bromoethane

CAS#:74-96-4
1-(2-chloroethoxy)-3-methylphosphol-3-ene structure

1-(2-chloroetho...

CAS#:50982-88-2

~%

1-ethyl-3-methyl-2,5-dihydro-1λ5-phosphole 1-oxide structure

1-ethyl-3-methy...

CAS#:7529-24-0
1,3-Dimethyl-2,5-dihydro-1H-phosphole 1-oxide structure

1,3-Dimethyl-2,...

CAS#:15450-79-0
Detail
Literature: Arbuzov, B. A.; Vizel', A. O.; Shchukina, L. I.; Giniyatullin, R. S. Doklady Chemistry, 1980 , vol. 253, p. 371 - 374 Dokl. Akad. Nauk SSSR Ser. Khim., 1980 , vol. 253, # 4 p. 879 - 883

 Synonyms

1-Oxo-1-methoxy-3-methyl-3-phospholene
3-Phospholene,1-methoxy-3-methyl-,1-oxide
1-methoxy-3-methyl-3-phospholene 1-oxide
1-methoxy-3-methyl-2,5-dihydro-1H-phosphole 1-oxide
1-Methoxy-3-methyl-1-oxo-1-phospha-cyclopenten-(3)
2,5-dihydro-1-methoxy-3-methyl-1H-phosphole 1-oxide
1-oxo-1-methoxy-3-methylphosphol-3-ene
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