Synthesis of Atabrine Analogs Having Various Aliphatic α-Substituents in the Side Chain1

…, RS Yost, HG Walker, CR Hauser

Index: Levine; Hauser Journal of the American Chemical Society, 1944 , vol. 66, p. 1768

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Citation Number: 13

Abstract

D-Gala-L-gulo-octito1.-A solution of 2.0 g. of D-gala+ gulo-octose in 50 cc. of water was agitated at 80'with Raney nickel and hydrogen under a pressure of 100 atmospheres for four hours; the catalyst was removed by filtration and the filtrate, which did not reduce Fehling solution, was concentrated in vacuo to dryness. The crystalline residue was dissolved in 3 cc. of warm water and the solution was diluted with IO cc. of alcohol; upon cooling, dusters ...

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