Tetrahedron Letters

Synthesis of 1-benzoyl-3-alkylthioureas by transamidation under microwave in dry media

H Márquez, ER Pérez, AM Plutı́n, M Morales, A Loupy

Index: Marquez, Heiddy; Perez, Eduardo R.; Plutin, Ana M.; Morales, Margarita; Loupy, Andre Tetrahedron Letters, 2000 , vol. 41, # 11 p. 1753 - 1756

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Citation Number: 22

Abstract

1-Benzoyl-3, 3-diethylthiourea was transamidated with several amines to the corresponding 1-benzoyl-3-alkylthioureas in open vessels under microwave irradiation using a domestic oven. The syntheses were performed in solvent-free conditions on potassium fluoride impregnated alumina. Yields were dramatically improved in comparison with classical heating under the same conditions.

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Synthesis of 1-benzoyl-3-alkylthioureas by transamidation under microwave in dry media

Abstract

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