The Nitration of 5-Methyl-2-thenoic Acid1

E Campaigne, HG Grose

Index: Campaigne; Grose Journal of the American Chemical Society, 1951 , vol. 73, p. 3812

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Citation Number: 13

Abstract

Discussion 5-Methyl-2-thenoic acid has been nitrated by RinkesJ2 using acetic anhydride and fuming nitric acid at-5 to-loo, to give as the main product (sic) 4-nitro-5-methyl-2-thenoic acid and small quantities of 5-nitro-2-methylthiophene and 3, 5-dinitro-2-methylthiophene. This reaction has been repeated in this work using red fuming nitric acid (trial I), and pure, colorless nitric acid (trial 11), each with acetic anhydride at-5 to-10'. The results are given ...

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