Tetrahedron letters

An efficient and cost-effective preparation of di-O-acetyl-D-rhamnal

JN Miller, R Pongdee

Index: Miller, Justin N.; Pongdee, Rongson Tetrahedron Letters, 2013 , vol. 54, # 24 p. 3185 - 3187

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Abstract

We have developed a synthetic route to the frequently utilized deoxysugar building block di- O-acetyl-d-rhamnal originating from the inexpensive starting material methyl α-d- glucopyranoside. Our approach proceeds in five steps with minimal column chromatography purification needed to afford the title compound in good overall yield.

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