Journal of the American Chemical Society

STUDIES ON POLYMERIZATION AND RING FORMATION. XVII. FRIEDEL-CRAFTS SYNTHESES WITH THE POLYANHYDRIDES OF THE DIBASIC ACIDS

JW Hill

Index: Hill Journal of the American Chemical Society, 1932 , vol. 54, p. 4105

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Citation Number: 15

Abstract

4106 JULIAN W. HILL Vol. 54 anhydride for six hours. The excess acetic anhydride and the acetic acid formed in the reaction were removed by distillation in vacuo up to 120 O bath temperature. The resulting polyanhydride" was dissolved in 400 cc. of warm, dry benzene. Three hundred grams of anhydrous aluminum chloride was suspended in 1500 cc. of dry benzene contained in a 3-necked 3-liter flask fitted with a reflux condenser and a ...

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