Hydrogen-bonding sheets in crystals for chirality recognition: synthesis and application of (2S, 3S)-2, 3-dihydroxy-and (2S, 3S)-2, 3-dibenzyloxy-1, 4-bis ( …
Y Kobayashi, Y Kokubo, T Aisaka, K Saigo
Index: Kobayashi, Yuka; Kokubo, Yasushi; Aisaka, Takamitsu; Saigo, Kazuhiko Tetrahedron Asymmetry, 2008 , vol. 19, # 21 p. 2536 - 2541
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Citation Number: 19
Abstract
Two enantiopure bis (hydroxyamino) compounds were successfully prepared from dialkyl tartrate by a chiral-pool method and applied as basic resolving agents in the enantioseparation of 2-arylpropanoic acids and arylglycolic acids.(2S, 3S)-2, 3-Dihydroxy-1, 4-bis (hydroxyamino) butane (2S, 3S)-1a could moderately recognize the chirality of the 2- arylpropanoic acids, while (2S, 3S)-2, 3-dibenzyloxy-1, 4-bis (hydroxyamino) butane (2S, ...
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