The Journal of Organic Chemistry

Approaches to the preparation of silyl cations

N Wang, JR Hwu, EH White

Index: Wang, Naelong; Hwu, Jih Ru; White, Emil H. Journal of Organic Chemistry, 1991 , vol. 56, # 1 p. 471 - 475

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Citation Number: 10

Abstract

(22) Rodriguez, J.; Thesis, Facult6 des Sciences et Techniques de St JBrBme, Marseille, France, 1984. (23) For preparation of the Vilsmeier reagent 111, see: Bredereck, H.; Bredereck, K. Chem. Ber. 1961,94,2278. I11 13C NMR (CDClJ 178,64, 62,lO 41,27, 39,05, 18,31; 31P NMR (H3P01) -7,31. (24) 'H NMR (CDCl,, 200 MHz) 6 2.84 (1 H, s), 2.30 (1 H, ddd, J = 16.2,8.6, 1.4 Hz), 2.14 (1 H, dd, J = 16.2, 8.6 Hz), 1.53 (1 H, dt, J = 16.4, 2.1 Hz), ...

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