Synthesis and activity of optical isomers of nipradilol.
M SHIRATSUCHI, K KAWAMURA, T AKASHI…
Index: Shiratsuchi; Kawamura; Akashi; Ishihama; Nakamura; Takenaka Chemical and Pharmaceutical Bulletin, 1987 , vol. 35, # 9 p. 3691 - 3698
Full Text: HTML
Citation Number: 15
Abstract
Four optical isomers of nipradilol (NIP) were prepared from (3R)-or (3S)-3, 4-dihydro-8- hydroxy-3-nitroxy-2H-1-benzopyran by glycidylation and amination, and evaluated for β- blocking and vasodilating activities. The order of potency of β-blocking activity was S, R- NIP>> S, S-NIP> R, R-NIP>> R, S-NIP. As regards vasodilating activity, S, R-NIP and R, R- NIP were more potent than S, S-NIP and R, S-NIP.
Related Articles:
[Golden, Kathryn C.; Gregg, Brian T.; Quinn, John F. Tetrahedron Letters, 2010 , vol. 51, # 31 p. 4010 - 4013]
[Leftheris, Katerina; Goodman, Murray Journal of Medicinal Chemistry, 1990 , vol. 33, # 1 p. 216 - 223]
[Kurimura; Takemoto; Achiwa Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 10 p. 2590 - 2596]
[Nelson,W.L. et al. Journal of Organic Chemistry, 1977 , vol. 42, p. 1006 - 1012]
[Wirz, Beat; Schmid, Rudolf; Foricher, Joseph Tetrahedron: Asymmetry, 1992 , vol. 3, # 1 p. 137 - 142]