Synthetic communications

Preparation of Methyl N??Substituted Carbamates from Amides through N??Chloroamides

GA Hiegel, TJ Hogenauer

Index: Hiegel, Gene A.; Hogenauer, Tyrone J. Synthetic Communications, 2005 , vol. 35, # 15 p. 2091 - 2098

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Citation Number: 12

Abstract

N??Chloramides are easily prepared from amides using trichloroisocyanuric acid [TCICA; 1,3,5??trichloro??1,3,5??triazine??2,4,6??(1H,3H,5H)??trione; C 3 Cl 3 N 3 O 3 ], a stable solid.11. Hiegel , GA , Hogenauer , TJ and Lewis , JC 2005. Preparation of N??chloroamides using trichloroisocyanuric acid. Synth. Commun., 35(15): 2099–2105. [Taylor & Francis Online], [Web of Science ®] View all references Treatment of N??chloroamides with aqueous hydroxide gives amines with ...

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