Synthesis

A new approach to the synthesis of the nonpeptide NOP receptor Antagonist J-113397

A Sulima, J Folk, AE Jacobson, KC Rice

Index: Synthesis, , # 10 p. 1547 - 1553

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Citation Number: 4

Abstract

... The last two steps of the synthesis involved reductive amination of compound 8 and the reduction of the ester ... solution of 12 (0.67 g, 4.7 mmol) in CH 2 Cl 2 (5 mL) was added p-toluenesulfonyl chloride ... 2 (7 mL) followed by addition of Et 3 N (0.72 mL, 5.17 mmol) at 5-10 °C. The ...

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A new approach to the synthesis of the nonpeptide NOP receptor Antagonist J-113397

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