Solid??Phase Reactive Chromatography (SPRC): A New Methodology for Wittig and Horner–Emmons Reactions on a Column under Microwave Irradiation

SC Dakdouki, D Villemin, N Bar

Index: Dakdouki, Saada C.; Villemin, Didier; Bar, Nathalie European Journal of Organic Chemistry, 2010 , # 2 p. 333 - 337

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Citation Number: 9

Abstract

Abstract A new methodology named solid-phase reactive chromatography (SPRC), which combines reaction, separation, and purification into a single unit for the preparation of small samples, is described. This method was illustrated in the synthesis of some natural bioactive compounds, namely, methoxylated analogues of resveratrol, alkylresorcinols, and 5-aryl-2, 4- pentadienoates, over a column of alumina-KF under microwave irradiation by using the ...

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