Synthesis of [4-2H2]-,(4R)[4-2H1]-and (4S)[4-2H1]-4-(methylnitrosamino)-1-(3'-pyridyl)-1-butanone, c-4 deuteriated isotopomers of the procarcinogen nnk

T Pathak, NF Thomas, M Akhtar, D Gani

Index: Tetrahedron, , vol. 46, # 5 p. 1733 - 1744

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Citation Number: 16

Abstract

... Download full text in PDF. Tetrahedron Vol. ... The residue was dissolved in minimum amount of water and applied to a column of Amberlite IR45 (OH) (100 ml settled volume). ... C-2); 30.1 (C-3); 28.9 (CH3); 16.9 (C-4). m/z (EI): 101 (M+, 100); 100 (32); 99 (54); 71 (16); 46 (86); 43 (62 ...