Toxic Fluorine Compounds. V. 1 ι-Fluoronitriles and ι-Fluoro-ι'-nitroalkanes

FLM Pattison, WJ Cott, WC Howell…

Index: Pattison et al. Journal of the American Chemical Society, 1956 , vol. 78, p. 3484,3485

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Citation Number: 16

Abstract

Condensation of Phenylacetaldehyde, Benzaldehyde and Ammonia.-After concentration of the ethanolic solution of the condensation products, 9.70 g. of solid, mp 110- 160", was collected from the residue diluted with an equal volume of ether. The crude basic material during the ether extraction yielded an additional 10.35 g., mp 90-145'. The rest of the material was distilled. The first fraction, bp 106-107° (14 mm.), n% 1.5393, weighed 2.13 g. and was identified as ...