The Journal of Organic Chemistry

Reactions of. alpha.-alkoxy-. alpha.,. beta.-unsaturated carbonyl compounds

J Quick, R Jenkins

Index: Quick,J.; Jenkins,R. Journal of Organic Chemistry, 1978 , vol. 43, p. 2275 - 2277

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Citation Number: 16

Abstract

Conclusion Conditions have been optimized to form the greatest amount of difluorobenze product. Under the following conditions: temperature,-78" C; fluorination schedule, 10/20/30; and fluorine to substrate ratio, 3; a maximum yield of 19.7% monofluorinated product was obtained. Despite the relatively high yield of desired products, there was no meta isomer found; however, measurable amounts of the meta isomer were observed in the ...