Nucleophilic cleavage reactions of cyclic and acyclic. alpha.-diazo-. beta.-ketophosphoryl compounds

H Tomioka, N Toriyama, Y Izawa

Index: Tomioka,H. et al. Journal of Organic Chemistry, 1977 , vol. 42, p. 552 - 554

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Citation Number: 3

Abstract

Catalyst prepared in methanol. Black ma-H:! initial pressure, ambient temperature. of 100 mmol of HY. terial prepared in DMF did not effect hydrogenation in DMF. lower grade chemicals and were used directly from the bottles without further purification. Palladium chloride was from Research Organic Chemicals; nickel acetate was from Fisher Scientific. All organic chemicals were analyzed for purity by gas chromatography prior to use. Liquid ...