The Journal of Organic Chemistry

Acid-catalyzed addition of secondary amines to cyclopropyl ketones. Mass spectra of some cyclic aminobutyrophenones

J Yovell, D Hirsch, S Sarel

Index: Yovell,J. et al. Journal of Organic Chemistry, 1977 , vol. 42, p. 850 - 855

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Citation Number: 7

Abstract

850 J. Org. Chem., Vol. 42, No. 5, 1977 Yovell, Hirsch, and Sarel authentic sample. The aqueous layer was acidified (hydrochloric acid) and extracted (ether). Evaporation of ether gave 0.41 g (68%) of diphenylacetic acid (13). Recrystallization of 13 from benzene gave colorless granules, mp 147-148" C. The melting point and IR spectrum of 13 were in good agreement with those of an authentic sample.