One??Pot Synthesis of 4??Alkoxybenzo [c] thiophenes
T Akbarzadeh, A Shafiee
Index: Akbarzadeh, Tahmineh; Shafiee, Abbas Synthetic Communications, 2004 , vol. 34, # 8 p. 1455 - 1462
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Abstract
Useful procedures for the synthesis of aryl alkyl ethers via aromatization of α,β??unsaturated cyclic ketones involve: dehydrogenation of 2??cyclohexen??1??one parts in polycylic compounds over palladium black in refluxing ethanol followed by methylation of the corresponding phenol with dimethyl sulfate,11. Turner , RB and Meschino , JA 1958. Assignment of the sixth hydroxyl group and a structural correlation with strophanthidin. J. Am. Chem. Soc., 80: 4862–4865.
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