The Journal of Organic Chemistry

Preparation and Diels-Alder reaction of (1E)-1, 3-dimethoxybutadiene

P Dowd, W Weber

Index: Dowd, Paul; Weber, William Journal of Organic Chemistry, 1982 , vol. 47, # 24 p. 4774 - 4777

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Citation Number: 14

Abstract

'H NMR spectra were recorded at 60 MHz with a Hitachi R-24 spectrometer. Measurements were made in CDC13 solution containing tetramethylsilane as an internal standard and in DzO with the sodium salt of 3-(trimethylsilyl) propanesulfonic acid (DSS) as the intemal standard. IR spectra were measured as KBr pellets and recorded on an IR-27 Shimadzu spectrophotometer. UV spectra were measured with Hitachi spectrometer, Model 124. ...