Regiospecific synthesis of arenesulfonamide derivatives of 3, 5-diamino-1, 2, 4-triazole

…, JE Dunbar, SW Snider, AP Vinogradoff

Index: Kleschick, William A.; Dunbar, Joseph E.; Snider, Sigrid W.; Vinogradoff, Anna P. Journal of Organic Chemistry, 1988 ,  vol. 53,  # 13  p. 3120 - 3122

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Citation Number: 5

Abstract

" IR and NMR spectral data recorded for all compounds were consistent with the assigned structure. Satisfactory analytical data (* 0.40% for C, H, N, C1, S) were reported for all new compounds listed in the table.* See the Experimental Section for a detailed description of the procedure. Experimental procedure A was found to be superior in this instance due to facilitating the removal of a byproduct, 2-(methylthio) nitrobenzene, by trituration with