The Reaction of Nitrous Acid with O-Alkylhydroxylamines1

JE Leffler, AA Bothner-By

Index: Leffler; Bothner-By Journal of the American Chemical Society, 1951 , vol. 73, p. 5473

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Citation Number: 7

Abstract

BY ET MCBEE, JF HIGGINS AND 0. R. PIERCE Although Henrya prepared ethyl 2- chlorocyanoacetate by chlorination of ethyl cyanoacetate, the 2, 2-dichloro compound has never been reported. This compound was desired as an intermediate for the preparation of a s-triazine. Chlorination of the ester at 140'produced the dichloro compound conveniently and in good yield. The preparation of the corresponding triazine by the method of McBee, ...

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