Thermal decomposition of amine oxides to olefins and dialkylhydroxylamines

AC Cope, TT Foster, PH Towle

Index: Cope; Foster; Towle Journal of the American Chemical Society, 1949 , vol. 71, p. 3929,3933

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Citation Number: 124

Abstract

Anal. Calcd. for C~~H~BN~OT: C, 44.14; H, 5.13. Found: C, 43.90; H, 4.91. The picrylsulfonate was obtained from amine and pic- rylsulfonic acid in isopropyl alcohol. After recrystalliza- tion from ethanol containing a little water, the melting point was 194.5-195" (dec.). Anal. Calcd. for CILH~~N~O~S: C, 36.73; H, 4.11. Found: C, 36.97; H, 4.22. Cyclobutene from Cyclobutyltrimethylammonium Hy- droxide.-Willstatter and von Schmaedel" prepared cyclobutene from ...

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