Total synthesis of ionomycin using ring-opening strategies

M Lautens, JT Colucci, S Hiebert, ND Smith…

Index: Organic Letters, , vol. 4, # 11 p. 1879 - 1882

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Citation Number: 110

Abstract

... Volume: Page: ... Organic Letters. ... S)-BINAP, toluene, 65 °C, 1.1 equiv of DIBAL-H (added over 20 h); (B) (a) DMSO, (COCl) 2 , NEt 3 , CH 2 Cl 2 , −78 °C; (b) PhMe, DIBAL-H, −78 °C; (c) THF, KHMDS, PMBCl; (C) O 3 , MeOH/CH 2 Cl 2 , −78 °C then NaBH 4 , rt; (D ...

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