Elektroreduktion organischer Verbindungen, 1. Kondensationsreaktionen des Acetonitrils mit Hilfe elektrogenerierter Basen

L Kistenbrügger, P Mischke, J Voß…

Index: Kistenbruegger, Lothar; Mischke, Peter; Voss, Juergen; Wiegand, Gabriele Liebigs Annalen der Chemie, 1980 , # 3 p. 461 - 471

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Abstract

Abstract Die elektrochemische Reduktion von Benzoesäureestern in wasserfreiem Acetonitril liefert Benzoylacetonitril (2). Aus Phenylglyoxylsäure-methylester (5) entsteht unter gleichen Bedingungen 3-Cyan-2-hydroxy-2-phenylpropionsäure-methylester (7).— Analog können aus N, N-Dialkylthiobenzamiden 8 β-Dialkylaminozimtsäurenitrile 9 erhalten werden. Aus N, N-Dimethylbenzamid (10) entsteht β-Dimethylaminozimtsäurenitril (9a) ...

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