Liebigs Annalen der Chemie

Conversion of Alcohols into Primary Amines, a New Mitsunobu Version of Gabriel??type Synthesis

E S̀lusarska, A Zwierzak

Index: Slusarska, Elzbieta; Zwierzak, Andrzej Liebigs Annalen der Chemie, 1986 , # 2 p. 402 - 405

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Citation Number: 5

Abstract

Primare und sekundare Alkohole liefern die entsprechenden Amin-hydrochloride 3 mit guten Ausbeuten (60-85%), wenn sie unter milden Bedingungen mit N- (Diethoxyphosphory1)-carbamidsaure-tert-butylester (1) in Gegenwart von Azodicarbonsaure-diethylester1Triphe-nylphosphan umgesetzt und danach die entstandenen N-Alkyl-N-(diethoxyphosphory1) carb-amidsaureester 2 mit gasformigem ...

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