Synthesis of N-thietan-3-yl-. alpha.-oxo nitrogen heterocycles from iminothioethers. A novel transformation

…, JJ McNally, ZG Hajos, RA Sawyers

Index: Press, Jeffery B.; McNally, James J.; Hajos, Zoltan G.; Sawyers, Rebecca A. Journal of Organic Chemistry, 1992 , vol. 57, # 23 p. 6335 - 6339

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Citation Number: 13

Abstract

DMF-d7) 6: 8.68 (e, 1 H), 7.35 (m, 5 HI, 5.95 (8, 1 HI, 5.11 (e, 2 H), 4.61 (d, J= 10 Hz, 2 H), 3.75 (e, 3 H), 3.68 (m, 2 H).'%-NMR (CDC13) 6: 169.34 (d, J= 3 Hz), 156.32, 136.31, 128.22, 127.78, 127.70, 66.69, 61.79 (d, J= 4 Hz), 52.09, 37.38 (d, J= 156 Hz). 31P-NMR 6: 22.64. FAB HRMS: calcd for C12H17N07P (MH+) 318.0741, found 318.0743.

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