Versatile Synthesis of Acylfuranones by Reaction of Acylketenes with α??Hydroxy Ketones: Application to the One??Step Multicomponent Synthesis of Cadiolide B and …

PA Peixoto, A Boulangé, S Leleu…

Index: European Journal of Organic Chemistry, , # 16 p. 3316 - 3327

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Citation Number: 6

Abstract

... European Journal of Organic Chemistry. ... The combined organic layers were then dried with MgSO 4 , filtered and concentrated under vacuum. ... solid in 98 % yield (8.5 g, 34 mmol), mp 75 °C. 1 H NMR (300 MHz, CDCl 3 ): δ = 1.63 (s, 3 H), 1.64 (s, 3 H), 2.57 [A(ABX), J AB = 21.9 ...

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