Acetopentamethylbenzene1

LI Smith, IM Webster, C Guss

Index: Smith; Webster; Guss Journal of the American Chemical Society, 1937 , vol. 59, p. 1078,1080

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Abstract

I078 LEE~ RVIN SMITH, ISABELLA M. WEBSTER AND CYRUS ('xuss Vol. 59 by washing the chloroform solution twice with 2% hydrochloric acid, once with dilute sodium bicarbonate solution, and crystallization of the sirup, recovered from the dried extract; from ether- petroleum ether at 0'. After one recrystallization from 90% ethanol, the acetate rotated+ 13.4" in chloroform and melted at 98.5-99'(corr.) alone or mixed with pure@-tetraacetate ...

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