2, 4, 4, 5, 7, 7, 8, 8, 9, 9, 9-Undecafluoro-2, 5-bis (trifluoromethyl)-3, 6-dioxanonyl methacrylate

O Paleta, J Paleček, J Michálek

Index: Paleta, Oldrich; Palecek, Jiri; Michalek, Jiri Journal of Fluorine Chemistry, 2002 , vol. 114, # 1 p. 51 - 53

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Citation Number: 12

Abstract

The title monomer (4) was prepared from the trimer of hexafluoropropene-1, 2-oxide, 2, 4, 4, 5, 7, 7, 8, 8, 9, 9, 9-undecafluoro-2, 5-bis (trifluoromethyl)-3, 6-dioxanonanoyl fluoride (1), via methyl ester 2 that was reduced by sodium borohydride to the corresponding alkanol 3, which was finally acylated by methacryloyl chloride.