Preparation and Characterization of [5??13C]??(2S, 4R)??Leucine and [4??13C]??(2S, 3S)??Valine− Establishing Synthetic Schemes to Prepare Any Site??Directed …

AHG Siebum, WS Woo…

Index: European Journal of Organic Chemistry, , # 23 p. 4664 - 4678

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Citation Number: 14

Abstract

... European Journal of Organic Chemistry. ... The organic layer was dried with MgSO 4 and the solvents were evaporated. The resulting raw product was purified by column chromatography (PE/E). Yield: 90 % (2.1 g). 1 H NMR (200 MHz, CDCl 3 ): δ = 1.25 (t, 3 J H,H = 7 Hz, 3 H, CH ...

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