Journal of the American Chemical Society
CONDENSATIONS AND RING CLOSURES IN THE NAPHTHALENE SERIES. IV. A SYNTHESIS OF ACEPHENANTHRENE
LF Fieser, MA Peters
Index: Fieser; Peters Journal of the American Chemical Society, 1932 , vol. 54, p. 4373,4378
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Citation Number: 13
Abstract
The possibility of preparing a still higher benzolog of acenaphthene by repeating the series of reactions used in the above syntheses was examined briefly. Condensed with succinic anhydride in nitrobenzene solution, tetrahydroacephenanthrene gave in good yield a keto acid which probably has the structure of X. This is inferred from the fact that sub-