Azidomethyl phenyl sulfide. A synthon for NH2

BM Trost, WH Pearson

Index: Trost, Barry M.; Pearson, William H. Journal of the American Chemical Society, 1981 , vol. 103, # 9 p. 2483 - 2485

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Citation Number: 65

Abstract

& $ a Grignard reagent prepared directly in normal fashion with Mg. Lithiation performed with n-butyllithium, except for entry 9, in which case sec-butyllithium was employed. Anhydrous magnesium bromide added. Anhydrous magnesium bromide added. combustion analysis and/or high-resolution mass spectroscopy;---indicates triazene not isolated but directly converted to amine. e Yield based upon the titer of the solution of the ...