The Journal of Organic Chemistry

Quaternary Derivatives of Nitrogen-Mustards1

T Nogrady, KM Vagi

Index: Nogrady,T.; Vagi,K.M. Journal of Organic Chemistry, 1962 , vol. 27, p. 2270 - 2271

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Citation Number: 2

Abstract

6.0 I I I 1 1 1 I 1 1 2 3 4 5 6 7 8 ... Fig. 1 .-The hydrolysis of 8-N,N-dimethylaminoethyl hydrogen phthalate at 75.5“, 0 ; and of methyl hydrogen phthalate at 109”, 0 (Ref. 6). ... Experimental 8-N,N-Dimethylaminoethyl Hydrogen Phthalate.- Phthalic anhydride (7.4 g., 0.05 mole) and 17.8 g. (0.2 mole) dimethylaminoethanol were placed in a 250-ml. three- necked round-bottomed flask equipped with a mechanical stirrer. The mixture was stirred at room temperature for ...