Chemosphere

A simple method for the preparation of dichlorocatechols

NH Kirsch, HJ Stan

Index: Kirsch, Nils H.; Stan, H.-J. Chemosphere, 1994 , vol. 28, # 1 p. 131 - 138

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Abstract

Abstract Dichlorocatechols (DCC) are common metabolites in the aerobic degradation of dichlorobenzenes. Their synthesis is therefore possible either enzymatically, or chemically by several two-step-syntheses starting from cycloalkanones or suitable dichlorophenols. A modified ultrasonic Reimer/Tiemann reaction and subsequent Dakin oxidation was used to prepare 3, 5-DCC and 4, 5-DCC. A new UV-photoradical single step synthesis of 3, 4- ...

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