Applications of microwave in organic synthesis: an improved one-step synthesis of metallophthalocyanines and a new modified microwave oven for dry …

D Villemin, M Hammadi, M Hachemi, N Bar

Index: Villemin, Didier; Hammadi, Mohamed; Hachemi, Messaoud; Bar, Nathalie Molecules, 2001 , vol. 6, # 10 p. 831 - 844

Full Text: HTML

Citation Number: 42

Abstract

Abstract: Metallophthalocyanine complexes are obtained quickly and efficiently by the reaction of phthalodinitrile with hydrated metallic salts without solvent and under microwave irradiation. The use of a modified commercial microwave oven to perform this type of reactions under dry conditions is described. Metallophthalocyanines and metallododecachlorophthalocyanines of some divalent metals can be also obtained from ...