Convenient Deuteration of Bromo Aromatic Compounds by Reductive Debromination with Sodium Amalgam in CH3OD

Y Miura, H Oka, E Yamano…

Index: Miura, Yozo; Oka, Hiroyuki; Yamano, Eiji; Morita, Masanori Journal of Organic Chemistry, 1997 , vol. 62, # 4 p. 1188 - 1190

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Citation Number: 18

Abstract

Deuterated compounds provide conclusive information on the proton assignments of 1H NMR and ESR spectra and play important roles in kinetic and mechanism studies and in the biochemical field. 1 However, the desired deuterated compounds, particularly partly deuterated compounds, with high isotopic purities are still difficult to prepare and require many steps in their preparation, starting from commercially available, but expensive ...

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