Synthetic communications

Improved Yields in the Synthesis of Spin??Labeled Fatty Acids

J Mravljak, S Pečar

Index: Mravljak, Janez; Pecar, Slavko Synthetic Communications, 2004 , vol. 34, # 20 p. 3763 - 3771

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Citation Number: 3

Abstract

Abstract Paramagnetic amide side products (6a–g) have been isolated from the reaction mixture in the synthesis of spin??labeled fatty acids of the doxyl type. After their hydrolysis to the corresponding acid, 7, the overall yield of spin??labeled fatty acids is significantly increased compared with published procedures.