McMurry intermolecular cross-coupling between an ester and a ketone: scope and limitations

S Sabelle, J Hydrio, E Leclerc, C Mioskowski…

Index: Tetrahedron Letters, , vol. 43, # 20 p. 3645 - 3648

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Citation Number: 31

Abstract

... Tetrahedron Letters. Volume 43, Issue 20, 13 May 2002, Pages 3645–3648. ... steps for the synthesis of chemiluminescent probes 1and 2. (i) R=H, 2-nitrophenyl sulfuryl chloride, THF, 2 h; R=NO 2 : 2,4-dinitrophenyl sulfuryl chloride, THF, 2 h; (ii) (PhO) 3 P, O 3 , −78 to 20°C, CH 2 ...