Synthesis of some α, β??unsaturated sulphones with potential acaricidal properties
M Gerstenfeld, PA Van Zwieten…
Index: Gerstenfeld,M. et al. Recueil des Travaux Chimiques des Pays-Bas, 1963 , vol. 82, p. 275 - 281
Full Text: HTML
Citation Number: 4
Abstract
The intermediate carboxylic acid V (R= H) was not isolated as it spontaneously decarboxylated to yield I. The relatively low yield (22%) of the condensation reaction is probably due to the instability of 4-chlorophenylsulphonylacetic acid, which partly decarboxylates during the condensation. Baliah and co-workers 6 also report low yields for this type of condensation reaction.
Related Articles:
[Springer, Dane M; Luh, Bing Yu; Goodrich, Jason T; Bronson, Joanne J Bioorganic and medicinal chemistry, 2003 , vol. 11, # 2 p. 281 - 291]
[Burton, Andrew J.; Cardwell, Kevin S.; Fuchter, Matthew J.; Lindvall, Mika K.; Patel, Rajnikant; Packham, Terry W.; Prodger, Jeremy C.; Schilling, Mark B.; Walker, Matthew D. Tetrahedron Letters, 2003 , vol. 44, # 30 p. 5653 - 5656]
[Aldous,F.A.B. et al. Journal of Medicinal Chemistry, 1974 , vol. 17, p. 1100 - 1111]
[Werbel; Elslager; Islip; Closier Journal of Medicinal Chemistry, 1977 , vol. 20, # 12 p. 1569 - 1572]
[Beilstein; Kuhlberg Justus Liebigs Annalen der Chemie, 1869 , vol. 152, p. 238]