Organometallics

Synthesis and coordination chemistry of N, N-diallylbispidine

H Cui, R Goddard, KR Pörschke

Index: Cui, Huiling; Goddard, Richard; Poerschke, Klaus-Richard Organometallics, 2011 , vol. 30, # 22 p. 6241 - 6252

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Citation Number: 11

Abstract

The synthesis of 3, 7-diallyl-3, 7-diazabicyclo [3.3. 1] nonane (C7H12N2allyl2, 3) has been revisited, and several hitherto undetected byproducts have been identified. Pure 3 and these byproducts were isolated by both prep-GC and column chromatography. Monoprotonated 3 in the form of the PF6 salt [(C7H13N2allyl2] PF6 (9) and the addition complexes of 3 to Ni (acac) 2 and CuI,(C7H12N2allyl2) Ni (acac) 2 (10) and {(C7H12N2allyl2) Cu (μ-I)} 2 (11), ...

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