First total synthesis of macrosphelides C and F

Y Kobayashi, HP Acharya

Index: Tetrahedron Letters, , vol. 42, # 15 p. 2817 - 2820

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Citation Number: 24

Abstract

... Tetrahedron Letters. Volume 42, Issue 15, 9 April 2001, Pages 2817–2820. ... The standard procedure 16 involving the following steps of (i) Cl 3 C 6 H 2 COCl, Et 3 N, THF; (ii) filtration; (iii) slow addition to DMAP in toluene, produced the 14-oxo lactone 13 in 35–42% yield, while ...