Synthesis and Solid??State NMR Studies of P??Vinylbenzylphosphonic Acid

…, JO Durand, F Carré, GF Lanneau…

Index: Frantz, Richard; Durand, Jean-Olivier; Carre, Francis; Lanneau, Gerard F.; Le Bideau, Jean; Alonso, Bruno; Massiot, Dominique Chemistry - A European Journal, 2003 , vol. 9, # 3 p. 770 - 775

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Citation Number: 21

Abstract

Abstract P-Vinylbenzylphosphonic acid (2) was synthesized and crystallized in two phases A and B. The latter phase was easily converted into the former. Both phases were investigated by IR and solid-state 31 P and 1 H NMR spectroscopy, and X-ray crystallography. The use of recently developed NMR methods has enabled us to increase the usually poor resolution of solid-state 1 H spectra. This gave additional insights on the proton environments. In ...

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