The Synthesis of Some Compounds Related to 3-Amino-1-propanethiol1

DS Tarbell, DA Buckley, PP Brownlee…

Index: Tarbell,D.S. et al. Journal of Organic Chemistry, 1964 , vol. 29, p. 3314 - 3319

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Citation Number: 8

Abstract

We found that boron trifluoride etherate was a better catalyst for the formation of the thiazine G than sulfuric acid; the former gave a 75% yield of G, and, in addition, dibenzyl sulfide and K-benzylbenzamide were isolated and identified from the boron fluoride reaction. With sulfuric acid as catalyst, the yield of thiazine was 5570 starting with the tertiary alcohol, but only 15% starting with the unsaturated compound F; the latter yielded much material ...