Journal of Pharmacy and Pharmacology

THE USE OF S??ALKYL??N??PHENYLTHIURONIUM PICRATES, STYPHNATES AND PICROLONATES FOR THE CHARACTERISATION OF ALKYL HALIDES

J Thomas, WA Baker

Index: Thomas,J.; Baker,W.A. Journal of Pharmacy and Pharmacology, 1960 , vol. 12, p. 460 - 465

Full Text: HTML

Citation Number: 1

Abstract

Both the nature of the halide and of the alkyl radical influence the time required for any particular alkyl halide to react with thiourea and different times of reaction have been recommended for chlorides, bromides and iodides1y3. To rationalise the method, a number of solvents and conditions have been investigated. Ethanol (absolute, 95 and 50 per cent) and acetone (80 and 50 per cent) were used for refluxing times varying from 5 minutes to ...