The Journal of Organic Chemistry

Synthesis of methyl 14-methyl-cis-8-hexadecenoate and 14-methyl-cis-8-hexadecen-1-ol. Sex attractant of Trogoderma inclusum

JI DeGraw, JO Rodin

Index: DeGraw,J.I.; Rodin,J.O. Journal of Organic Chemistry, 1971 , vol. 36, p. 2902 - 2903

Full Text: HTML

Citation Number: 10

Abstract

NOTES J. Org. Chem., Vol. $6, No. 19, 1971 2903 spectrum was identical with that of material prepared by lithium aluminum hydride reduction of methyl 6-methy1octanoate. a 6- Methyl-1-octanal (4).-To 450 ml of pyridine was slowly added 45 g of chromic acid with stirring and maintdnence of the temperature below 30". The resulting yellow precipitate was treated with 1 1. of hexane and quickly filtered. The solid was washed with hexane and ...